Salicylic acid was treated with guaiacol and phosphorus oxychloride at100℃ and the guaiacol salicylate obtained was o— acetylated to give2— methoxyphenyl o— acetylsalicylate. 其方法是水杨酸与愈创木酚混合,加入三氯氧磷在100℃反应,制得愈创木酚水杨酸酯,再乙酰化即得到乙酰水杨酸愈创木酚酯。
Guaiacol \Guai"a*col\, n. [Guaiacum + -ol.] (Chem.) A colorless liquid, {C7H8O2}, with a peculiar odor. It is the methyl ether of pyrocatechin, and is obtained by distilling guaiacum from wood-tar creosote, and in other ways. It has been used in the past for treating pulmonary tuberculosis. [Webster 1913 Suppl.]